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TITLE:  Determination of oxytetracycline in bovine kidney and medicated milk replacer by liquid chromatography
 
AUTHORS:  Kijak PJ;Cope CV;Pedersoli WM;
 
YEAR:  1999
 
JOURNAL ABBREV:  J AOAC Int
 
MONTH:  Nov
 
TYPE:  JOUR
 
REFMAN INDEX:  80
 
JOURNAL FULL:  Journal of AOAC International
 
VOLUME:  82
 
ISSUE:  6
 
START PAGE:  1329
 
END PAGE:  1333
 
KEYWORDS:  analysis;Animals;Anti-Bacterial Agents;Cattle;chemistry;Chromatography;Chromatography,Liquid;Diet;Food;Food Additives;Kidney;methods;Milk;Oxytetracycline;veterinary;Veterinary Medicine;
 
ABSTRACT:  Improvements and optimization of AOAC INTERNATIONAL Official Method 995.09 for the detection of oxytetracycline in bovine kidney at the new U.S. tolerance of 12 ppm are reported. Recoveries from kidney fortified at 4 concentrations over the range of 3-40 ppm averaged 84-98%. Results from the kidney of a calf fed medicated milk replacer containing oxytetracycline are also reported. Additionally, adaptation of this method to the detection of oxytetracycline in medicated milk replacer is discussed
 
AFFILIATIONS:  U.S. Food and Drug Administration, Center for Veterinary Medicine, Laurel, MD 20708, USA
 
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